Bee Gee Maurice Gibb has died in hospital in Miami, Florida.
The 53-year-old had been in a critical condition after suffering a heart attack during an operation to remove an intestinal blockage after he collapsed at his Florida home last week.
His wife Yvonne and his two children had been with him at the Mount Sinai Medical Centre the surgery on Thursday night.
Maurice Gibb
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A statement released by his family said: "It is with great sadness and sorrow that we regretfully announce the passing of Maurice Gibb this morning.
"His love and enthusiasm and energy for life remain an inspiration to all of us. We will all deeply miss him." The family statement said that he died at 1.00 a.m.
Yesterday, his family and fans outside the hospital were hopeful that he was showing signs of recovery as he opened his eyes for a brief time and squeezed his daughter's hand..
As a member of the Bee Gees, Maurice Gibb had been one of the best-known faces in British showbusiness for the last four decades. He, his twin Robin and elder brother Barry, started their singing careers in the 1950s, earning their name from a previous incarnation as the Brothers Gibb.
Their hits include the soundtrack to the film of the disco phenomenon , Saturday Night Fever, in 1977 and a sequel, Stayin' Alive, in 1983.
Saturday Night Feversaw some of the group's most successful tracks such as Stayin' Alive, How Deep Is Your Loveand Night Fever. One of their most successful collaborations was with Motown legend Diana Ross and Chain Reactionin January 1986.
Gibb, the bass guitarist and keyboard player in the group, had well-documented problems with alcohol. He met his first wife, the singer Lulu, in the BBC canteen. They married in 1969 but divorced four years later.